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Use este identificador para citar o ir al link de este elemento: http://hdl.handle.net/1843/46660
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Campo DCValorIdioma
dc.creatorMariana Cristina da Silvapt_BR
dc.creatorRicardo Mathias Orlandopt_BR
dc.creatorAdriana Ferreira Fariapt_BR
dc.date.accessioned2022-10-26T20:23:55Z-
dc.date.available2022-10-26T20:23:55Z-
dc.date.issued2016-
dc.citation.volume1461pt_BR
dc.citation.spage27pt_BR
dc.citation.epage34pt_BR
dc.identifier.doihttps://doi.org/10.1016/j.chroma.2016.07.063pt_BR
dc.identifier.issn0021-9673pt_BR
dc.identifier.urihttp://hdl.handle.net/1843/46660-
dc.description.resumoThis work presents a new method by electrical matrix solid phase dispersion for the extraction and clean-up of marbofloxacin, ofloxacin, norfloxacin, ciprofloxacin, enrofloxacin, difloxacin and sarafloxacin in bovine milk. Composition and pH of the eluent, applied electrical potential and polarity were optimized by experimental designs. The combination of the chromatographic and electrophoretic mechanisms allowed the extraction and clean-up in one step with low organic solvent consumption, high extraction throughput and elution automation. Linearity, precision, trueness and limit of quantification were evaluated and provided values in accordance with other methods recently developed for the analysis of fluoroquinolones in milk. This technique proved to be promising for the extraction and clean-up of ionizable analytes in different milk matrices.pt_BR
dc.description.sponsorshipCNPq - Conselho Nacional de Desenvolvimento Científico e Tecnológicopt_BR
dc.description.sponsorshipFAPEMIG - Fundação de Amparo à Pesquisa do Estado de Minas Geraispt_BR
dc.description.sponsorshipCAPES - Coordenação de Aperfeiçoamento de Pessoal de Nível Superiorpt_BR
dc.description.sponsorshipINCT – Instituto nacional de ciência e tecnologia (Antigo Instituto do Milênio)pt_BR
dc.languageengpt_BR
dc.publisherUniversidade Federal de Minas Geraispt_BR
dc.publisher.countryBrasilpt_BR
dc.publisher.departmentICX - DEPARTAMENTO DE QUÍMICApt_BR
dc.publisher.initialsUFMGpt_BR
dc.relation.ispartofJournal of Chromatography Apt_BR
dc.rightsAcesso Restritopt_BR
dc.subjectElectrical field assisted matrix solid phase dispersionpt_BR
dc.subjectExtractionpt_BR
dc.subjectClean-uppt_BR
dc.subjectFluoroquinolonespt_BR
dc.subjectBovine milkpt_BR
dc.subjectUHPLC–MS/MSpt_BR
dc.subjectUltra-high performance liquid chromatographypt_BR
dc.subject.otherExtração (Química)pt_BR
dc.subject.otherLeitept_BR
dc.subject.otherSolventes orgânicospt_BR
dc.subject.otherAnálise cromatográficapt_BR
dc.subject.otherExtração por solventespt_BR
dc.subject.otherPreparação de amostra (Química)pt_BR
dc.subject.otherCromatografia liquida de alta eficienciapt_BR
dc.titleElectrical field assisted matrix solid phase dispersion as a powerful tool to improve the extraction efficiency and clean-up of fluoroquinolones in bovine milkpt_BR
dc.typeArtigo de Periódicopt_BR
dc.url.externahttps://www.sciencedirect.com/science/article/pii/S0021967316309852pt_BR
dc.identifier.orcidhttps://orcid.org/0000-0002-3862-1211pt_BR
dc.identifier.orcidhttps://orcid.org/0000-0002-7320-4907pt_BR
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