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Please use this identifier to cite or link to this item: http://hdl.handle.net/1843/57067
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dc.creatorJúlia Cristina Soarespt_BR
dc.creatorKisla Prislen Felix Siqueirapt_BR
dc.creatorRoberto Luiz Moreirapt_BR
dc.creatorAnderson Diaspt_BR
dc.date.accessioned2023-07-27T18:12:07Z-
dc.date.available2023-07-27T18:12:07Z-
dc.date.issued2016-
dc.citation.volume678pt_BR
dc.citation.spage57pt_BR
dc.citation.epage64pt_BR
dc.identifier.doihttps://doi.org/10.1016/j.jallcom.2016.03.291pt_BR
dc.identifier.issn0925-8388pt_BR
dc.identifier.urihttp://hdl.handle.net/1843/57067-
dc.description.resumoPhase-pure monoclinic NdLuO3 interlanthanides were successfully synthesized from hydrothermal-derived precursors. LuO(OH) and Nd(OH)3 materials were firstly obtained by hydrothermal synthesis at 250 °C, for 24 h. X-ray diffraction, micro-Raman spectroscopy, scanning and transmission electron microscopies were employed to investigate the thermal behavior of these precursors and NdLuO3 interlanthanide up to 1600 °C. It was observed that LuO(OH) and Nd(OH)3 were converted to cubic lanthanide oxides below 1000 °C. Cubic Nd2O3 has changed to the monoclinic structure at 1000 °C, followed by reaction with cubic Lu2O3 at 1400 °C to produce monoclinic NdLuO3. Phase-pure monoclinic (C2/m space group, #12) interlanthanide was then produced at 1600 °C for the first time, as confirmed by all the employed techniques. Phonon modes were additionally determined and assigned for this monoclinic structure.pt_BR
dc.description.sponsorshipCNPq - Conselho Nacional de Desenvolvimento Científico e Tecnológicopt_BR
dc.description.sponsorshipFAPEMIG - Fundação de Amparo à Pesquisa do Estado de Minas Geraispt_BR
dc.description.sponsorshipCAPES - Coordenação de Aperfeiçoamento de Pessoal de Nível Superiorpt_BR
dc.description.sponsorshipFINEP - Financiadora de Estudos e Projetos, Financiadora de Estudos e Projetospt_BR
dc.description.sponsorshipOutra Agênciapt_BR
dc.languageengpt_BR
dc.publisherUniversidade Federal de Minas Geraispt_BR
dc.publisher.countryBrasilpt_BR
dc.publisher.departmentICX - DEPARTAMENTO DE FÍSICApt_BR
dc.publisher.departmentICX - DEPARTAMENTO DE QUÍMICApt_BR
dc.publisher.initialsUFMGpt_BR
dc.relation.ispartofJournal of Alloys and Compoundspt_BR
dc.rightsAcesso Restritopt_BR
dc.subjectCeramicspt_BR
dc.subjectElectron microscopypt_BR
dc.subjectNanomaterialspt_BR
dc.subjectRaman spectroscopypt_BR
dc.subjectRare-earthpt_BR
dc.subject.otherCeramicapt_BR
dc.subject.otherMicroscopia eletronicapt_BR
dc.subject.otherMateriais nanoestruturadospt_BR
dc.subject.otherRaman, Espectroscopia dept_BR
dc.subject.otherCompostos de metais de terras raraspt_BR
dc.subject.otherMetais de terras raraspt_BR
dc.titleStructural and vibrational properties of phase-pure monoclinic NdLuO3 interlanthanides synthesized from nanostructured precursorspt_BR
dc.typeArtigo de Periódicopt_BR
dc.url.externahttps://www.sciencedirect.com/science/article/pii/S0925838816309008pt_BR
dc.identifier.orcidhttps://orcid.org/0000-0002-6344-3103pt_BR
dc.identifier.orcidhttps://orcid.org/0000-0001-6820-0269pt_BR
dc.identifier.orcidhttps://orcid.org/0000-0001-7413-1087pt_BR
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