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Please use this identifier to cite or link to this item: http://hdl.handle.net/1843/39654
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dc.creatorPatrícia Amaral Souza Tettept_BR
dc.creatorFabiano Aurélio da Silva Oliveirapt_BR
dc.creatorElba Nathália Corrêa Pereirapt_BR
dc.creatorGilsara Silvapt_BR
dc.creatorMaria Beatriz de Abreu Glóriapt_BR
dc.creatorChristian Fernandespt_BR
dc.date.accessioned2022-02-24T15:05:01Z-
dc.date.available2022-02-24T15:05:01Z-
dc.date.issued2016-
dc.citation.volume211pt_BR
dc.citation.spage130pt_BR
dc.citation.epage139pt_BR
dc.identifier.doi10.1016/j.foodchem.2016.05.036pt_BR
dc.identifier.issn03088146pt_BR
dc.identifier.urihttp://hdl.handle.net/1843/39654-
dc.description.resumoBee products can be produced in an environment contaminated by pesticides that can be transported by honey bees to the hive and incorporated into the honey. Therefore, rapid and modern methods to determine pesticide residues in honey samples are essential to guarantee consumers’ health. In this study, a simple multiresidue method for the quantification of 116 pesticides in honey is proposed. It involves the use of a modified QuEChERS procedure followed by UHPLC–MS/MS analysis. The method was validated according to the European Union SANCO/12571/2013 guidelines. Acceptable values were obtained for the following parameters: linearity, limit of detection (0.005 mg/kg) and limit of quantification (0.010 and 0.025 mg/kg), trueness (for the four tested levels the recovery assays values were between 70 and 120%), intermediate precision (RSD < 20.0%) and measurement uncertainty tests (<50.0%). The validated method was applied for determination of 100 honey samples from five states of Brazil.pt_BR
dc.description.sponsorshipCNPq - Conselho Nacional de Desenvolvimento Científico e Tecnológicopt_BR
dc.description.sponsorshipFAPEMIG - Fundação de Amparo à Pesquisa do Estado de Minas Geraispt_BR
dc.format.mimetypepdfpt_BR
dc.languageengpt_BR
dc.publisherUniversidade Federal de Minas Geraispt_BR
dc.publisher.countryBrasilpt_BR
dc.publisher.departmentFAR - DEPARTAMENTO DE ALIMENTOSpt_BR
dc.publisher.departmentFAR - DEPARTAMENTO DE PRODUTOS FARMACÊUTICOSpt_BR
dc.publisher.initialsUFMGpt_BR
dc.relation.ispartofFood Chemistrypt_BR
dc.rightsAcesso Abertopt_BR
dc.subjectPesticidespt_BR
dc.subjectHoneypt_BR
dc.subjectQuEChERSpt_BR
dc.subjectUHPLC-MS/MSpt_BR
dc.subjectProficiency testpt_BR
dc.subject.otherAgrotóxicospt_BR
dc.subject.otherMelpt_BR
dc.titleMulticlass method for pesticides quantification in honey by means of modified QuEChERS and UHPLC–MS/MSpt_BR
dc.typeArtigo de Periódicopt_BR
dc.url.externahttps://www.sciencedirect.com/science/article/pii/S0308814616307166pt_BR
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