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Please use this identifier to cite or link to this item: http://hdl.handle.net/1843/39655
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dc.creatorWarlley Pinheiro Evangelistapt_BR
dc.creatorTarliane Maria da Silvapt_BR
dc.creatorLetícia Rocha Guidipt_BR
dc.creatorPatrícia Amaral Souza Tettept_BR
dc.creatorRicardo Martins Duarte Byrropt_BR
dc.creatorPaula Santiago-Silvapt_BR
dc.creatorChristian Fernandespt_BR
dc.creatorMaria Beatriz de Abreu Glóriapt_BR
dc.date.accessioned2022-02-24T15:20:36Z-
dc.date.available2022-02-24T15:20:36Z-
dc.date.issued2016-
dc.citation.volume211pt_BR
dc.citation.spage100pt_BR
dc.citation.epage106pt_BR
dc.identifier.doi10.1016/j.foodchem.2016.05.035pt_BR
dc.identifier.issn03088146pt_BR
dc.identifier.urihttp://hdl.handle.net/1843/39655-
dc.description.resumoHistamine determination is relevant for fish safety, quality and trade. Recently a study by the European Union (EU) compared the Codex and the EU mandated methods for the analysis of histamine and observed that they underestimated and overestimated the results, respectively. To solve this problem, a simple and efficient procedure for the extraction and quantification of histamine by ion-pair HPLC method with post-column derivatization and fluorimetric detection is proposed. It was optimized and validated for the analysis of histamine in fish. The method attended the performance criteria established by Commission Decision 2002/657/CE. The method was also submitted to proficiency testing; uncertainty was calculated; and the stability of solutions and standards was investigated. There was no matrix effect. The LOD, LOQ, CCα and CCβ were fit for the purpose. The method was successfully used in the analyses of freshwater fish and fresh and canned tuna.pt_BR
dc.description.sponsorshipCNPq - Conselho Nacional de Desenvolvimento Científico e Tecnológicopt_BR
dc.description.sponsorshipFAPEMIG - Fundação de Amparo à Pesquisa do Estado de Minas Geraispt_BR
dc.format.mimetypepdfpt_BR
dc.languageengpt_BR
dc.publisherUniversidade Federal de Minas Geraispt_BR
dc.publisher.countryBrasilpt_BR
dc.publisher.departmentFAR - DEPARTAMENTO DE ALIMENTOSpt_BR
dc.publisher.departmentFAR - DEPARTAMENTO DE PRODUTOS FARMACÊUTICOSpt_BR
dc.publisher.initialsUFMGpt_BR
dc.relation.ispartofFood Chemistrypt_BR
dc.rightsAcesso Restritopt_BR
dc.subjectMatrix effectpt_BR
dc.subjectFishpt_BR
dc.subjectHistamine analysispt_BR
dc.subjectProficiency testpt_BR
dc.subjectUncertaintypt_BR
dc.subject.otherControle de qualidadept_BR
dc.subject.otherPeixespt_BR
dc.titleQuality assurance of histamine analysis in fresh and canned fishpt_BR
dc.typeArtigo de Periódicopt_BR
dc.url.externahttps://www.sciencedirect.com/science/article/pii/S0308814616307154?via%3Dihubpt_BR
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