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http://hdl.handle.net/1843/40863| Type: | Artigo de Periódico |
| Title: | Evaluation of the influence of extraction conditions on the isolation and identification of volatile compounds from cagaita (Eugenia dysenterica) using HS-SPME/GC-MS |
| Authors: | Mauro Ramalho Silva Gustavo Hernandes Bueno Raquel Linhares Bello de Araújo Inayara Cristina Alves Lacerda Lucas Gomes de Freitas Harriman Alley de Morais Rodinei Augusti Júlio Onésio Ferreira Melo |
| Abstract: | The objective of this study was to explore the extraction and identification of volatile organic compounds (VOCs) present in cagaita fruit (Eugenia dysenterica). Parameters such as type of extraction fiber, agitation, extraction time and extraction temperature were investigated. Initially, the VOCs were extracted using headspace solid-phase microextraction. Then, the compounds were identified using gas chromatography coupled to mass spectrometry. Results revealed the presence of at least 26 different compounds and the polyacrylate (PA) fiber promoted the extraction of a larger number of VOCs. Regarding the PA fiber, the most efficient extraction was achieved using a 50 rpm agitation at 45 ºC for 30 min. The majority were monoterpenes (34.64%) and esters (36.28%). An increase in the extraction temperature promoted the isolation of more VOCs when using carboxen/polydimethylsiloxane (CAR/PDMS) and divinylbenzene/carboxen/polydimethylsiloxane (DVB/CAR/PDMS) fibers. However, these fibers allowed the isolation of a smaller number of VOCs. The extraction time and agitation had no significant influence. |
| Subject: | Cagaita Compostos orgânicos voláteis Eugenia dysenterica |
| language: | eng |
| metadata.dc.publisher.country: | Brasil |
| Publisher: | Universidade Federal de Minas Gerais |
| Publisher Initials: | UFMG |
| metadata.dc.publisher.department: | FAR - DEPARTAMENTO DE ALIMENTOS ICX - DEPARTAMENTO DE QUÍMICA |
| Rights: | Acesso Aberto |
| metadata.dc.identifier.doi: | 10.21577/0103-5053.20180187 |
| URI: | http://hdl.handle.net/1843/40863 |
| Issue Date: | Feb-2019 |
| metadata.dc.url.externa: | https://www.scielo.br/j/jbchs/a/bqM6LHT9Zjfvbm7bzBRkXnw/?lang=en |
| metadata.dc.relation.ispartof: | Journal of the Brazilian Chemical Society |
| Appears in Collections: | Artigo de Periódico |
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