Please use this identifier to cite or link to this item: http://hdl.handle.net/1843/46409
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dc.creatorSunday Joseph Olusegunpt_BR
dc.creatorErico Tadeu Fraga Freitaspt_BR
dc.creatorLuciano Roni Silva Larapt_BR
dc.creatorHumberto Osório Stumpfpt_BR
dc.creatorNelcy Della Santina Mohallempt_BR
dc.date.accessioned2022-10-19T18:19:37Z-
dc.date.available2022-10-19T18:19:37Z-
dc.date.issued2019-
dc.citation.volume45pt_BR
dc.citation.issue7 Part Apt_BR
dc.citation.spage8734pt_BR
dc.citation.epage8743pt_BR
dc.identifier.doihttps://doi.org/10.1016/j.ceramint.2019.01.197pt_BR
dc.identifier.issn0272-8842pt_BR
dc.identifier.urihttp://hdl.handle.net/1843/46409-
dc.description.resumoSynthesis of CoFe2O4 nanoparticles was carried out using a co-precipitation method. The resulting precipitate was dried by using conventional method (oven), and spray drying process. The products obtained from the two drying processes were calcined at 500 and 700 °C; and characterized by powder X-ray diffraction (XRD), scanning electron microscopy (SEM) transmission electron microscopy (TEM), and N2 gas adsorption technique. Magnetic measurements were performed on a SQUID magnetometer. The magnetic saturation value (76 emu g−1) of the spray dried cobalt ferrite calcined at 700 °C (SD-700) was higher than its corresponding oven-dried sample. The as-received spray dried CoFe2O4 nanoplates (SD-100) has the highest BET specific surface area (138 m2 g−1), while the oven-dried sample calcined at 700 °C (OD-700) has the lowest area (47 m2 g−1). Cobalt ferrite samples obtained from the two drying processes were briefly applied to adsorb methylene blue solution as a cationic dye model to know the effect of drying process on the adsorption of dye. The studies showed that all the spray dried samples performed better in adsorbing methylene blue (MB) solution. Energy-filtered TEM (EFTEM) analysis that was carried out on SD-700 ascertained the adsorption of MB on its surface.pt_BR
dc.description.sponsorshipCNPq - Conselho Nacional de Desenvolvimento Científico e Tecnológicopt_BR
dc.description.sponsorshipFAPEMIG - Fundação de Amparo à Pesquisa do Estado de Minas Geraispt_BR
dc.description.sponsorshipOutra Agênciapt_BR
dc.format.mimetypepdfpt_BR
dc.languageengpt_BR
dc.publisherUniversidade Federal de Minas Geraispt_BR
dc.publisher.countryBrasilpt_BR
dc.publisher.departmentICX - DEPARTAMENTO DE QUÍMICApt_BR
dc.publisher.initialsUFMGpt_BR
dc.relation.ispartofCeramics internationalpt_BR
dc.rightsAcesso Restritopt_BR
dc.subjectSpray drying processpt_BR
dc.subjectSpecific surface areapt_BR
dc.subjectMethylene blue adsorptionpt_BR
dc.subjectMagnetic propertiespt_BR
dc.subject.otherNanopartículaspt_BR
dc.subject.otherRaios Xpt_BR
dc.subject.otherDifraçãopt_BR
dc.subject.otherMicroscopia eletrônicapt_BR
dc.subject.otherCobaltopt_BR
dc.subject.otherFerritapt_BR
dc.subject.otherAdsorçãopt_BR
dc.subject.otherCarbenos (Compostos de metileno)pt_BR
dc.titleEffect of drying process and calcination on the structural and magnetic properties of cobalt ferritept_BR
dc.typeArtigo de Periódicopt_BR
dc.url.externahttps://www.sciencedirect.com/science/article/pii/S0272884219302147pt_BR
dc.identifier.orcidhttps://orcid.org/0000-0002-2479-0540pt_BR
dc.identifier.orcidhttps://orcid.org/0000-0002-8509-8662pt_BR
dc.identifier.orcidhttps://orcid.org/0000-0001-7756-0987pt_BR
dc.identifier.orcidhttps://orcid.org/0000-0002-9094-4536pt_BR
Appears in Collections:Artigo de Periódico

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