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http://hdl.handle.net/1843/48757| Tipo: | Artigo de Periódico |
| Título: | Efficient extraction method using magnetic carbon nanotubes to analyze cocaine and benzoylecgonine in breast milk by GC/MS |
| Autor(es): | Rosimeire Resende dos Santos Maria José Nunes Paiva Júlio César Veloso Philippe Serp Zenilda de Lourdes Cardeal Helvécio Costa Menezes |
| Resumo: | Aim: The increasing use of cocaine (COC) during breastfeeding has led to growing concern about exposure of infants. Therefore, to study this exposure, a new method to analyze COC and benzoylecgonine in breast milk was developed. Methodology: A new extraction method was used for the first time to analyze COC and its major metabolite, benzoylecgonine, in breast milk using magnetic carbon nanotubes partially doped with nitrogen. Results: The calibration curves were linear in the range 5.0–180.0 ng ml-1. The limit of quantification was 5.0 ng ml-1. Coefficients of variation were between 3.2 and 13.9%. Recovery was between 89.6 and 99.2%. Conclusion: The proposed method is simple, efficient and suitable to determine analytes in breast milk. |
| Assunto: | Amamentação Leite humano Análise Cocaína Cromatografia de gás Espectrometria de massa Nanotubos de carbono |
| Idioma: | eng |
| País: | Brasil |
| Editor: | Universidade Federal de Minas Gerais |
| Sigla da Instituição: | UFMG |
| Departamento: | FAR - DEPARTAMENTO DE ANÁLISES CLÍNICAS E TOXICOLÓGICAS ICX - DEPARTAMENTO DE QUÍMICA |
| Tipo de Acesso: | Acesso Restrito |
| Identificador DOI: | https://doi.org/10.4155/bio-2017-0140 |
| URI: | http://hdl.handle.net/1843/48757 |
| Data do documento: | 2017 |
| metadata.dc.url.externa: | https://www.future-science.com/doi/abs/10.4155/bio-2017-0140?journalCode=bio |
| metadata.dc.relation.ispartof: | Bioanalysis |
| Aparece nas coleções: | Artigo de Periódico |
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