Multiclass method for pesticides quantification in honey by means of modified QuEChERS and UHPLC–MS/MS

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dc.creatorPatrícia Amaral Souza Tette
dc.creatorFabiano Aurélio da Silva Oliveira
dc.creatorElba Nathália Corrêa Pereira
dc.creatorGilsara Silva
dc.creatorMaria Beatriz de Abreu Glória
dc.creatorChristian Fernandes
dc.date.accessioned2022-02-24T15:05:01Z
dc.date.accessioned2025-09-09T01:30:06Z
dc.date.available2022-02-24T15:05:01Z
dc.date.issued2016
dc.description.sponsorshipCNPq - Conselho Nacional de Desenvolvimento Científico e Tecnológico
dc.description.sponsorshipFAPEMIG - Fundação de Amparo à Pesquisa do Estado de Minas Gerais
dc.format.mimetypepdf
dc.identifier.doi10.1016/j.foodchem.2016.05.036
dc.identifier.issn03088146
dc.identifier.urihttps://hdl.handle.net/1843/39654
dc.languageeng
dc.publisherUniversidade Federal de Minas Gerais
dc.relation.ispartofFood Chemistry
dc.rightsAcesso Aberto
dc.subjectAgrotóxicos
dc.subjectMel
dc.subject.otherPesticides
dc.subject.otherHoney
dc.subject.otherQuEChERS
dc.subject.otherUHPLC-MS/MS
dc.subject.otherProficiency test
dc.titleMulticlass method for pesticides quantification in honey by means of modified QuEChERS and UHPLC–MS/MS
dc.typeArtigo de periódico
local.citation.epage139
local.citation.spage130
local.citation.volume211
local.description.resumoBee products can be produced in an environment contaminated by pesticides that can be transported by honey bees to the hive and incorporated into the honey. Therefore, rapid and modern methods to determine pesticide residues in honey samples are essential to guarantee consumers’ health. In this study, a simple multiresidue method for the quantification of 116 pesticides in honey is proposed. It involves the use of a modified QuEChERS procedure followed by UHPLC–MS/MS analysis. The method was validated according to the European Union SANCO/12571/2013 guidelines. Acceptable values were obtained for the following parameters: linearity, limit of detection (0.005 mg/kg) and limit of quantification (0.010 and 0.025 mg/kg), trueness (for the four tested levels the recovery assays values were between 70 and 120%), intermediate precision (RSD < 20.0%) and measurement uncertainty tests (<50.0%). The validated method was applied for determination of 100 honey samples from five states of Brazil.
local.publisher.countryBrasil
local.publisher.departmentFAR - DEPARTAMENTO DE ALIMENTOS
local.publisher.departmentFAR - DEPARTAMENTO DE PRODUTOS FARMACÊUTICOS
local.publisher.initialsUFMG
local.url.externahttps://www.sciencedirect.com/science/article/pii/S0308814616307166

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