Synephrine - a potential biomarker for orange honey authenticity

dc.creatorPatrícia Amaral Souza Tette
dc.creatorLetícia Rocha Guidi
dc.creatorEsther Margarida Alves Ferreira Bastos
dc.creatorChristian Fernandes
dc.creatorMaria Beatriz de Abreu Glória
dc.date.accessioned2022-02-22T10:34:38Z
dc.date.accessioned2025-09-09T00:50:56Z
dc.date.available2022-02-22T10:34:38Z
dc.date.issued2017
dc.description.sponsorshipCAPES - Coordenação de Aperfeiçoamento de Pessoal de Nível Superior
dc.format.mimetypepdf
dc.identifier.doi10.1016/j.foodchem.2017.02.108
dc.identifier.issn03088146
dc.identifier.urihttps://hdl.handle.net/1843/39556
dc.languageeng
dc.publisherUniversidade Federal de Minas Gerais
dc.relation.ispartofFood Chemistry
dc.rightsAcesso Aberto
dc.subjectQuímica
dc.subjectCiência e Tecnologia de Alimentos
dc.subject.otherSynephrine
dc.subject.otherOrange honey
dc.subject.otherCitrus honey
dc.subject.otherHoney
dc.subject.otherBotanical origin
dc.subject.otherBiomarker
dc.subject.otherAmines
dc.titleSynephrine - a potential biomarker for orange honey authenticity
dc.typeArtigo de periódico
local.citation.epage533
local.citation.issue229
local.citation.spage527
local.description.resumoA LC-MS/MS method for synephrine as a biomarker for orange honey authenticity was developed and validated. The sample was extracted with 5% TCA and cleaned up with Florisil providing 83.7% recoveries. Ions transitions for quantification and identification were 168→135.0 and 168→107.0, respectively. The limits of detection and quantification were 0.66 and 1.0ng/g, respectively. Synephrine was detected in orange honey at levels from 79.2 to 432.2ng/g, but not in other monofloral honeys. It was also present in some wildflower honeys (9.4-236.5ng/g), showing contribution of citrus to this polyfloral honey. Results were confirmed by qualitative pollen analysis. No citrus pollen was detected in honey containing synephrine levels ≤43.8ng/g, suggesting that synephrine in honey is more sensitive compared to pollen analysis. Synephrine was found in citrus but not in other apiculture flowers. Therefore, synephrine is a botanical marker to differentiate and attest authenticity of orange honey.
local.publisher.countryBrasil
local.publisher.departmentFAR - DEPARTAMENTO DE ALIMENTOS
local.publisher.departmentFAR - DEPARTAMENTO DE PRODUTOS FARMACÊUTICOS
local.publisher.initialsUFMG
local.url.externahttps://pubmed.ncbi.nlm.nih.gov/28372211/

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