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http://hdl.handle.net/1843/39655| Type: | Artigo de Periódico |
| Title: | Quality assurance of histamine analysis in fresh and canned fish |
| Authors: | Warlley Pinheiro Evangelista Tarliane Maria da Silva Letícia Rocha Guidi Patrícia Amaral Souza Tette Ricardo Martins Duarte Byrro Paula Santiago-Silva Christian Fernandes Maria Beatriz de Abreu Glória |
| Abstract: | Histamine determination is relevant for fish safety, quality and trade. Recently a study by the European Union (EU) compared the Codex and the EU mandated methods for the analysis of histamine and observed that they underestimated and overestimated the results, respectively. To solve this problem, a simple and efficient procedure for the extraction and quantification of histamine by ion-pair HPLC method with post-column derivatization and fluorimetric detection is proposed. It was optimized and validated for the analysis of histamine in fish. The method attended the performance criteria established by Commission Decision 2002/657/CE. The method was also submitted to proficiency testing; uncertainty was calculated; and the stability of solutions and standards was investigated. There was no matrix effect. The LOD, LOQ, CCα and CCβ were fit for the purpose. The method was successfully used in the analyses of freshwater fish and fresh and canned tuna. |
| Subject: | Controle de qualidade Peixes |
| language: | eng |
| metadata.dc.publisher.country: | Brasil |
| Publisher: | Universidade Federal de Minas Gerais |
| Publisher Initials: | UFMG |
| metadata.dc.publisher.department: | FAR - DEPARTAMENTO DE ALIMENTOS FAR - DEPARTAMENTO DE PRODUTOS FARMACÊUTICOS |
| Rights: | Acesso Restrito |
| metadata.dc.identifier.doi: | 10.1016/j.foodchem.2016.05.035 |
| URI: | http://hdl.handle.net/1843/39655 |
| Issue Date: | 2016 |
| metadata.dc.url.externa: | https://www.sciencedirect.com/science/article/pii/S0308814616307154?via%3Dihub |
| metadata.dc.relation.ispartof: | Food Chemistry |
| Appears in Collections: | Artigo de Periódico |
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