Synthesis of 25X-BOMes and 25X-NBOHs (X = H, I, Br) for pharmacological studies and as reference standards for forensic purposes

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dc.creatorWellington Alves de Barros
dc.creatorMarcelo Pereira Queiroz
dc.creatorLeonardo da Silva Neto
dc.creatorGraziele Martins Borges
dc.creatorFelipe Terra Martins
dc.creatorÂngelo de Fátima
dc.date.accessioned2024-11-01T22:56:27Z
dc.date.accessioned2025-09-08T22:50:52Z
dc.date.available2024-11-01T22:56:27Z
dc.date.issued2021
dc.description.sponsorshipCNPq - Conselho Nacional de Desenvolvimento Científico e Tecnológico
dc.description.sponsorshipFAPEMIG - Fundação de Amparo à Pesquisa do Estado de Minas Gerais
dc.description.sponsorshipCAPES - Coordenação de Aperfeiçoamento de Pessoal de Nível Superior
dc.format.mimetypepdf
dc.identifier.doihttps://doi.org/10.1016/j.tetlet.2020.152804
dc.identifier.issn0040-4039
dc.identifier.urihttps://hdl.handle.net/1843/77795
dc.languageeng
dc.publisherUniversidade Federal de Minas Gerais
dc.relation.ispartofTetrahedron Letters
dc.rightsAcesso Aberto
dc.subjectQuímica legal
dc.subjectFenetilamina
dc.subjectPsicotrópicos
dc.subjectCromatografia de gás - Aplicações Forenses
dc.subjectAminas
dc.subjectAldeídos
dc.subject.otherPhenethylamines
dc.subject.otherReference standards
dc.subject.otherNBOMes
dc.subject.otherNBOHs
dc.titleSynthesis of 25X-BOMes and 25X-NBOHs (X = H, I, Br) for pharmacological studies and as reference standards for forensic purposes
dc.typeArtigo de periódico
local.citation.spage152804
local.citation.volume66
local.description.resumoAn expeditious method is reported for the synthesis of three NBOHs (25H-, 25I- and 25B-NBOH; 9–38% overall yield) and three NBOMes (25H-, 25I- and 25B-NBOMe; 7–33% overall yield) from salicylaldehyde and 2-methoxyaldehyde, respectively. The X-ray structures of 25H-, 25I- and 25B-NBOH.HCl were also determined. Our approach should provide a general entry for preparing such a class of substances for pharmacological and forensic purposes.
local.identifier.orcidhttps://orcid.org/0000-0002-3479-0720
local.identifier.orcidhttps://orcid.org/0000-0003-4554-9577
local.identifier.orcidhttps://orcid.org/0000-0002-2835-1094
local.identifier.orcidhttps://orcid.org/0000-0001-9004-0927
local.identifier.orcidhttps://orcid.org/0000-0003-2344-5590
local.publisher.countryBrasil
local.publisher.departmentICX - DEPARTAMENTO DE QUÍMICA
local.publisher.initialsUFMG
local.url.externahttps://www.sciencedirect.com/science/article/pii/S0040403920313289

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