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http://hdl.handle.net/1843/72115
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DC Field | Value | Language |
---|---|---|
dc.creator | Hugo Paul Collin | pt_BR |
dc.creator | Wallace Junio Reis | pt_BR |
dc.creator | Dennis Ulsøe Nielsen | pt_BR |
dc.creator | Anders Thyboe Lindhardt | pt_BR |
dc.creator | Marcelo Siqueira Valle | pt_BR |
dc.creator | Rossimiriam Pereira de Freitas | pt_BR |
dc.creator | Troels Skrydstrup | pt_BR |
dc.date.accessioned | 2024-07-30T19:31:10Z | - |
dc.date.available | 2024-07-30T19:31:10Z | - |
dc.date.issued | 2019 | - |
dc.citation.volume | 21 | pt_BR |
dc.citation.issue | 15 | pt_BR |
dc.citation.spage | 5775 | pt_BR |
dc.citation.epage | 5778 | pt_BR |
dc.identifier.doi | https://doi.org/10.1021/acs.orglett.9b01423 | pt_BR |
dc.identifier.issn | 1523-7052 | pt_BR |
dc.identifier.uri | http://hdl.handle.net/1843/72115 | - |
dc.description.resumo | Bench-stable tablets (COtabs) have been developed for the rapid and safe production of carbon monoxide. The tablets can be made in less than 5 min without the use of a glovebox and only require a stock solution of an amine base to liberate a specific quantity of CO in a two-chamber system. The COtabs were tested in five different carbonylation reactions and provided similar yields compared to literature procedures. Finally, a gram-scale reaction was conducted, as well as 13C-isotope labeling of the anticancer drug, olaparib. | pt_BR |
dc.description.sponsorship | CAPES - Coordenação de Aperfeiçoamento de Pessoal de Nível Superior | pt_BR |
dc.description.sponsorship | Outra Agência | pt_BR |
dc.language | eng | pt_BR |
dc.publisher | Universidade Federal de Minas Gerais | pt_BR |
dc.publisher.country | Brasil | pt_BR |
dc.publisher.department | ICX - DEPARTAMENTO DE QUÍMICA | pt_BR |
dc.publisher.initials | UFMG | pt_BR |
dc.relation.ispartof | Organic Letters | pt_BR |
dc.rights | Acesso Restrito | pt_BR |
dc.subject | Carbonylation | pt_BR |
dc.subject | Catalysts | pt_BR |
dc.subject | Inorganic carbon compounds | pt_BR |
dc.subject | Oxides | pt_BR |
dc.subject | Reagents | pt_BR |
dc.subject.other | Catalisadores | pt_BR |
dc.subject.other | Compostos de carbono | pt_BR |
dc.subject.other | Comportos inorgânicos | pt_BR |
dc.subject.other | Óxidos | pt_BR |
dc.subject.other | Testes químicos e reagentes | pt_BR |
dc.subject.other | Agentes antineoplásicos | pt_BR |
dc.title | COtab: expedient and safe setup for Pd-catalyzed carbonylation chemistry | pt_BR |
dc.type | Artigo de Periódico | pt_BR |
dc.url.externa | https://pubs.acs.org/doi/10.1021/acs.orglett.9b01423 | pt_BR |
dc.identifier.orcid | https://orcid.org/0000-0001-9483-7183 | pt_BR |
dc.identifier.orcid | https://orcid.org/0000-0001-7337-6488 | pt_BR |
dc.identifier.orcid | https://orcid.org/0000-0002-4521-5991 | pt_BR |
dc.identifier.orcid | https://orcid.org/0000-0001-8941-4899 | pt_BR |
dc.identifier.orcid | https://orcid.org/0000-0002-9759-9915 | pt_BR |
dc.identifier.orcid | https://orcid.org/0000-0001-6974-3724 | pt_BR |
dc.identifier.orcid | https://orcid.org/0000-0001-8090-5050 | pt_BR |
Appears in Collections: | Artigo de Periódico |
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