Please use this identifier to cite or link to this item: http://hdl.handle.net/1843/72115
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dc.creatorHugo Paul Collinpt_BR
dc.creatorWallace Junio Reispt_BR
dc.creatorDennis Ulsøe Nielsenpt_BR
dc.creatorAnders Thyboe Lindhardtpt_BR
dc.creatorMarcelo Siqueira Vallept_BR
dc.creatorRossimiriam Pereira de Freitaspt_BR
dc.creatorTroels Skrydstruppt_BR
dc.date.accessioned2024-07-30T19:31:10Z-
dc.date.available2024-07-30T19:31:10Z-
dc.date.issued2019-
dc.citation.volume21pt_BR
dc.citation.issue15pt_BR
dc.citation.spage5775pt_BR
dc.citation.epage5778pt_BR
dc.identifier.doihttps://doi.org/10.1021/acs.orglett.9b01423pt_BR
dc.identifier.issn1523-7052pt_BR
dc.identifier.urihttp://hdl.handle.net/1843/72115-
dc.description.resumoBench-stable tablets (COtabs) have been developed for the rapid and safe production of carbon monoxide. The tablets can be made in less than 5 min without the use of a glovebox and only require a stock solution of an amine base to liberate a specific quantity of CO in a two-chamber system. The COtabs were tested in five different carbonylation reactions and provided similar yields compared to literature procedures. Finally, a gram-scale reaction was conducted, as well as 13C-isotope labeling of the anticancer drug, olaparib.pt_BR
dc.description.sponsorshipCAPES - Coordenação de Aperfeiçoamento de Pessoal de Nível Superiorpt_BR
dc.description.sponsorshipOutra Agênciapt_BR
dc.languageengpt_BR
dc.publisherUniversidade Federal de Minas Geraispt_BR
dc.publisher.countryBrasilpt_BR
dc.publisher.departmentICX - DEPARTAMENTO DE QUÍMICApt_BR
dc.publisher.initialsUFMGpt_BR
dc.relation.ispartofOrganic Letterspt_BR
dc.rightsAcesso Restritopt_BR
dc.subjectCarbonylationpt_BR
dc.subjectCatalystspt_BR
dc.subjectInorganic carbon compoundspt_BR
dc.subjectOxidespt_BR
dc.subjectReagentspt_BR
dc.subject.otherCatalisadorespt_BR
dc.subject.otherCompostos de carbonopt_BR
dc.subject.otherComportos inorgânicospt_BR
dc.subject.otherÓxidospt_BR
dc.subject.otherTestes químicos e reagentespt_BR
dc.subject.otherAgentes antineoplásicospt_BR
dc.titleCOtab: expedient and safe setup for Pd-catalyzed carbonylation chemistrypt_BR
dc.typeArtigo de Periódicopt_BR
dc.url.externahttps://pubs.acs.org/doi/10.1021/acs.orglett.9b01423pt_BR
dc.identifier.orcidhttps://orcid.org/0000-0001-9483-7183pt_BR
dc.identifier.orcidhttps://orcid.org/0000-0001-7337-6488pt_BR
dc.identifier.orcidhttps://orcid.org/0000-0002-4521-5991pt_BR
dc.identifier.orcidhttps://orcid.org/0000-0001-8941-4899pt_BR
dc.identifier.orcidhttps://orcid.org/0000-0002-9759-9915pt_BR
dc.identifier.orcidhttps://orcid.org/0000-0001-6974-3724pt_BR
dc.identifier.orcidhttps://orcid.org/0000-0001-8090-5050pt_BR
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